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博碩士論文 etd-0725115-143720 詳細資訊
Title page for etd-0725115-143720
論文名稱
Title
數位影像相關法於Cr薄膜殘留應力的量測
Measurement of the Residual Stress in Cr-Film by Using DIC
系所名稱
Department
畢業學年期
Year, semester
語文別
Language
學位類別
Degree
頁數
Number of pages
118
研究生
Author
指導教授
Advisor
召集委員
Convenor
口試委員
Advisory Committee
口試日期
Date of Exam
2015-07-27
繳交日期
Date of Submission
2015-08-25
關鍵字
Keywords
鍍膜、數位影像相關法、殘留應力、鍍膜厚度、懸臂樑
digital image correlation, film thickness, residual stress, coating film, cantilever beam
統計
Statistics
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The thesis/dissertation has been browsed 5813 times, has been downloaded 1703 times.
中文摘要
以往學者在量測鍍薄膜於基板的殘留應力時,皆採用Stoney's equation,並假設鍍膜於基板接觸介面上之殘留應力為均勻分布,本論文之研究目的在藉由量測矽基板上鍍不同厚度之鉻薄膜後,鍍膜殘留應力的分佈情況,以及殘留應力與鍍膜厚度的關係,以探討殘留應力為均勻分布此假設之適當性。首先在以矽基板製成之懸臂樑鍍上固定厚度之Cr薄膜,透過量測懸臂樑因薄膜殘留應力導致的面外位移後,即可用修正後之Stoney's equation計算出薄膜殘留應力。面外位移的大小是使用數位影像相關法量測,且僅需使用單一CCD鏡頭。本論文共探討了三種鍍膜厚度,分別為1 μm、2 μm和3 μm,每種厚度有三個試片,每個試片上選擇九個不同測試點來量測殘留應力,以探討殘留應力的分步情況。研究結果顯示隨著薄膜厚度增加,殘留應力大小有下降的趨勢,結合實驗結果和統計理論顯示,薄膜厚度3 μm之殘留應力值小於薄膜厚度1 μm時之可靠度為86.5%;實驗結果也顯示殘留應力並非均勻分布,薄膜厚度為1 μm時其殘留應力分布比3 μm時更不均勻之可靠度為70.98%。
Abstract
In the past, if a researcher intended to measure the residual stress in a thin film coated on a substrate, the Stoney's equation was adopted and assumed that the residual stresses on the interface between film and substrate were distributed uniformity. The purpose of this thesis was to discuss the flexibility of previously mentioned uniformly distributed residual stresses assumption by investigating the distribution of residual stresses in different thickness of Cr film coated on a silicon substrate. Also, the relationship between the film thickness and the magnitude and distribution of residual stresses were studied. Firstly, a specific thickness of Cr film was coated on a cantilever beam made of silicon. Then, the residual stress can be calculated by using modified Stoney's equation and the measured out-of-plane deformation of the cantilever beam which were caused by film residual stresses. The out-of-plane deformation were measured by using digital image correlation technique with single CCD only. This thesis explored three coating thicknesses, which were 1 μm, 2 μm and 3 μm, respectively, and there were three specimens corresponded to each thickness. In order to investigate the distribution of residual stresses, the residual stresses at nine different test points on each specimen were determined. The results showed a trend that the magnitude of residual stress decreased with increasing film thickness. By combining the experimental results and statistical theory showed that the reliability of the magnitude of residual stress corresponding to 3 μm film thickness smaller than 1 μm film thickness was 86.5%. The results also showed that the residual stresses were distributed non-uniformity. The reliability of the residual stresses corresponding to 1 μm film thickness distributed more non-uniform than 3 μm film thickness was 70.98%.
目次 Table of Contents
謝誌 i
摘要 ii
Abstact iii
目錄 iv
表目錄 vii
圖目錄 viii
符號表 xi
第一章 緒論 1
1.1研究動機與目的 1
1.2文獻回顧 2
1.2.1數位影像相關法源起 2
1.2.2數位影像相關法三維量測之發展 4
1.2.3三維DIC之應用 5
1.2.4鍍薄膜基板薄膜殘留應力 6
1.3全文架構 9
第二章 基礎理論 10
2.1數位影像相關法 10
2.1.1影像圖片資訊 10
2.1.2影像重建 11
2.1.3物體平面變形理論 12
2.1.4影像相關原理 13
2.1.5影像特徵搜尋 14
2.1.6求取最佳位移函數 15
2.2旋轉座標理論 17
2.3鍍薄膜基板殘留應力 18
第三章 實驗方法 31
3.1實驗儀器與設備 31
3.1.1 硬體儀器 31
3.1.2 軟體設備 33
3.2實驗步驟 34
3.2.1 矽基板與鉻薄膜的規劃 34
3.2.2 矽基板表面影像擷取與分析 35
3.3三維數位影像相關法量測理論推導 36
3.3.1公式推導 36
3.3.2量測角度設定 39
3.3.3比例因子 39
3.3.4影像重建誤差 40
3.3.5量測範圍 42
3.4數位影像相關法三维位移量測誤差分析 42
3.4.1數位影像相關法的解析度和準確度 43
3.4.2剛體位移和剛體旋轉的驗證 45
3.4.3分析結果的正確性 46
3.5應用懸臂樑於鍍薄膜基板薄膜殘留應力之量測 47
3.5.1鍍薄膜基板殘留應力公式推導 47
3.5.2誤差分析 48
第四章 結果與討論 68
4.1實驗結果 68
4.2面外位移量 69
4.3殘留應力的平均值 70
4.4殘留應力的均勻度 72
第五章 結論與未來展望 88
5.1結論 88
5.2未來展望 89
參考文獻 90
附錄 99
附錄一 99
附錄二 102
參考文獻 References
[1] 胡錦標, 精密光電技術. 台北, 台灣: 高立圖書有限公司, 1992.
[2] R. Daniel, K. J. Martinschitz, J. Keckes, and C. Mitterer, "The origin of stresses in magnetron-sputtered thin films with zone T structures," Acta Materialia, vol. 58, pp. 2621-2633, 2010.
[3] Q. Kong, L. Ji, H. Li, X. Liu, Y. Wang, J. Chen, et al., "Influence of substrate bias voltage on the microstructure and residual stress of CrN films deposited by medium frequency magnetron sputtering," Materials Science and Engineering: B, vol. 176, pp. 850-854, 2011.
[4] W. H. Peters and W. F. Ranson, "Digital imaging techniques in experimental stress analysis," Optical Engineering, vol. 21, pp. 213427-213427, 1982.
[5] M. A. Sutton, W. J. Wolters, W. H. Peters, W. F. Ranson, and S. R. McNeill, "Determination of displacements using an improved digital correlation method," Image and Vision Computing, vol. 1, pp. 133-139, 1983.
[6] T. C. Chu, W. F. Ranson, and M. A. Sutton, "Applications of digital-image-correlation techniques to experimental mechanics," Experimental Mechanics, vol. 25, pp. 232-244, 1985.
[7] M. A. Sutton, S. R. McNeill, J. Jang, and M. Babai, "Effects of subpixel image restoration on digital correlation error estimates," Optical Engineering, vol. 27, pp. 232-244, 1988.
[8] M. A. Sutton, C. Mingqi, W. H. Peters, Y. J. Chao, and S. R. McNeill, "Application of an optimized digital correlation method to planar deformation analysis," Image and Vision Computing, vol. 4, pp. 143-150, 1986.
[9] H. A. Bruck, S. R. McNeill, M. A. Sutton, and W. H. Peters, III, "Digital image correlation using Newton-Raphson method of partial differential correction," Experimental Mechanics, vol. 29, pp. 261-267, 1989.
[10] B. Pan and K. Li, "A fast digital image correlation method for deformation measurement," Optics and Lasers in Engineering, vol. 49, pp. 841-847, 2011.
[11] Y. Yuan, J. Huang, X. Peng, C. Xiong, J. Fang, and F. Yuan, "Accurate displacement measurement via a self-adaptive digital image correlation method based on a weighted ZNSSD criterion," Optics and Lasers in Engineering, vol. 52, pp. 75-85, 2014.
[12] R. Y. Tsai, "A versatile camera calibration technique for high-accuracy 3D machine vision metrology using off-the-shelf TV cameras and lenses," Robotics and Automation, IEEE Journal of, vol. 3, pp. 323-344, 1987.
[13] J. H. Vogel and D. Lee, "An automated two-view method for determining strain distributions on deformed surfaces," Journal of Materials Shaping Technology, vol. 6, pp. 205-216, 1988.
[14] Z. L. Kahn-Jetter and T. C. Chu, "Three-dimensional displacement measurements using digital image correlation and photogrammic analysis," Experimental Mechanics, vol. 30, pp. 10-16, 1990.
[15] P. F. Luo, Y. J. Chao, M. A. Sutton, and W. H. Peters, III, "Accurate measurement of three-dimensional deformations in deformable and rigid bodies using computer vision," Experimental Mechanics, vol. 33, pp. 123-132, 1993.
[16] K. Kawasue and T. Ishimatsu, "3-D measurement of moving particles by circular image shifting," Industrial Electronics, IEEE Transactions on, vol. 44, pp. 703-706, 1997.
[17] Z. Zhengyou, "A flexible new technique for camera calibration," Pattern Analysis and Machine Intelligence, IEEE Transactions on, vol. 22, pp. 1330-1334, 2000.
[18] C. Quan, C. J. Tay, and Y. H. Huang, "3-D deformation measurement using fringe projection and digital image correlation," Optik - International Journal for Light and Electron Optics, vol. 115, pp. 164-168, 2004.
[19] C. J. Tay, C. Quan, Y. H. Huang, and Y. Fu, "Digital image correlation for whole field out-of-plane displacement measurement using a single camera," Optics Communications, vol. 251, pp. 23-36, 2005.
[20] S. Roux, F. Hild, P. Viot, and D. Bernard, "Three-dimensional image correlation from X-ray computed tomography of solid foam," Composites Part A: Applied Science and Manufacturing, vol. 39, pp. 1253-1265, 2008.
[21] J. Harvent, B. Coudrin, L. Brèthes, J.-J. Orteu, and M. Devy, "Shape measurement using a new 3D-DIC algorithm that preserves sharp edges," Advancement of Optical Methods in Experimental Mechanics, vol. 3, pp. 69-76, 2014.
[22] 吳家勝, "數位影像相關法於三維變形量測之新應用," 機械與機電工程學系, 國立中山大學, 台灣,高雄, 2009.
[23] W. H. Peters, W. F. Ranson, M. A. Sutton, T. C. Chu, and J. Anderson, "Application of digital correlation methods to rigid body mechanics," Optical Engineering, vol. 22, pp. 226738-226738, 1983.
[24] Z. H. He, M. A. Sutton, W. F. Ranson, and W. H. Peters, "Two-dimensional fluid-velocity measurements by use of digital-speckle correlation techniques," Experimental Mechanics, vol. 24, pp. 117-121, 1984.
[25] W. Wu, W. H. Peters, 3rd, and M. E. Hammer, "Basic mechanical properties of retina in simple elongation," J Biomech Eng, vol. 109, pp. 65-7, 1987.
[26] G. Han, M. A. Sutton, and Y. J. Chao, "A study of stationary crack-tip deformation fields in thin sheets by computer vision," Experimental Mechanics, vol. 34, pp. 125-140, 1994.
[27] D. S. Dawicke and M. A. Sutton, "CTOA and crack-tunneling measurements in thin sheet 2024-T3 aluminum alloy," Experimental Mechanics, vol. 34, pp. 357-368, 1994.
[28] G. Han, M. A. Sutton, Y. J. Chao, and J. S. Lyons, "A study of stable crack growth in thin SEC specimens of 304 stainless steel by computer vision," Engineering Fracture Mechanics, vol. 52, pp. 525-555, 1995.
[29] G. Vendroux and W. G. Knauss, "Submicron deformation field measurements: Part 1. Developing a digital scanning tunneling microscope," Experimental Mechanics, vol. 38, pp. 18-23, 1998.
[30] G. Vendroux and W. G. Knauss, "Submicron deformation field measurements: Part 2. Improved digital image correlation," Experimental Mechanics, vol. 38, pp. 86-92, 1998.
[31] G. Vendnroux, N. Schmidt, and W. G. Knauss, "Submicron deformation field measurements: Part 3. Demonstration of deformation determinations," Experimental Mechanics, vol. 38, pp. 154-160, 1998.
[32] V. Tiwari, M. A. Sutton, S. R. McNeill, S. Xu, X. Deng, W. L. Fourney, et al., "Application of 3D image correlation for full-field transient plate deformation measurements during blast loading," International Journal of Impact Engineering, vol. 36, pp. 862-874, 2009.
[33] F. Grytten, H. Daiyan, M. Polanco-Loria, and S. Dumoulin, "Use of digital image correlation to measure large-strain tensile properties of ductile thermoplastics," Polymer Testing, vol. 28, pp. 653-660, 2009.
[34] P. Bing, X. Hui-min, H. Tao, and A. Asundi, "Measurement of coefficient of thermal expansion of films using digital image correlation method," Polymer Testing, vol. 28, pp. 75-83, 2009.
[35] M. Sebastiani, C. Eberl, E. Bemporad, and G. M. Pharr, "Depth-resolved residual stress analysis of thin coatings by a new FIB–DIC method," Materials Science and Engineering: A, vol. 528, pp. 7901-7908, 2011.
[36] W.-C. Wang, Y.-T. Chou, H.-Y. Chieh, and W. J. Sian, "Inspection of internal defects in cfrp circular tubes by three-dimensional digital image correction method," 15th International Conference on Experimental Mechanics 2012.
[37] M. Krottenthaler, C. Schmid, J. Schaufler, K. Durst, and M. Göken, "A simple method for residual stress measurements in thin films by means of focused ion beam milling and digital image correlation," Surface and Coatings Technology, vol. 215, pp. 247-252, 2013.
[38] D. Nowell, M. Kartal, and P. D. Matos, "Digital image correlation measurement of near‐tip fatigue crack displacement fields: constant amplitude loading and load history effects," Fatigue & Fracture of Engineering Materials and Structures, vol. 36, pp. 3-13, 2013.
[39] E. Fagerholt, T. Børvik, and O. Hopperstad, "Measuring discontinuous displacement fields in cracked specimens using digital image correlation with mesh adaptation and crack-path optimization," Optics and Lasers in Engineering, vol. 51, pp. 299-310, 2013.
[40] G. Gore, "On the properties of electro-deposited antimony," Philosophical Transactions of the Royal Society of London, vol. 148, pp. 185-197, 1858.
[41] E. J. Mills, "On Electrostriction," Proceedings of the Royal Society of London, vol. 26, pp. 504-512, 1877.
[42] G. G. Stoney, "The tension of metallic films deposited by electrolysis," Proceedings of the Royal Society of London. Series A, Containing Papers of a Mathematical and Physical Character, vol. 82, pp. 172-175, 1909.
[43] E. Klokholm, "An apparatus for measuring stress in thin films," Review of Scientific Instruments, vol. 40, pp. 1054-1058, 1969.
[44] B. C. Bell and D. A. Glocker, "Insitu measurements of film stress in AlN sputtered onto moving substrates," Journal of Vacuum Science & Technology A, vol. 9, pp. 2437-2441, 1991.
[45] W. Fang and J. A. Wickert, "Determining mean and gradient residual stresses in thin films using micromachined cantilevers," J. Micromech. Microeng., vol. 6, pp. 301–309, 1996.
[46] G. Moulard, G. Contoux, G. Gardet, G. Motyl, and M. Courbon, "An improved optical cantilever technique using image processing for measuring in situ stress in thin films," Surface and Coatings Technology, vol. 97, pp. 206-211, 1997.
[47] E. Chason, J. A. Floro, and L. B. Freund, "Extensions of the Stoney formula for substrate curvature to configurations with thin substrates or large deformations," Applied Physics Letters, vol. 74, 1999.
[48] Z. Suo, E. Y. Ma, H. Gieskove, and S. Wagner, "Mechanics of rollable and foldable film-on-foil electronics," J. of applied physics, vol. 74, pp. 1177-1179, 1999.
[49] C. L. Tien, C. C. Lee, and C. C. Jaing, "The measurement of thin film stress by using phase shifting interferometry," J. of Modern Optics, vol. 47, pp. 839-849, 2000.
[50] A. Ni, D. Sherman, R. Ballarini, H. Kahn, B. Mi, S. M. Phillips, et al., "Optimal design of multilayered polysilicon films for prescribed curvature," Journal of Materials Science, vol. 38, pp. 4169-4173, 2003.
[51] Y. Y. Hu and W. M. Hunag, "Elastic and elastic-plastic analysis of multilayerthin films:Closed-form solution," J. of applied physics, vol. 96, pp. 4154-4160, 2004.
[52] K. S. Chen, T. Y.-F. Chen, C. C. Chuang, and I. K. Lin, "Full-Field wafer level thin film stress measurement by phase-stepping shadow moiré," IEEE Trans. on Components and Packaging Tech, vol. 27, pp. 594-601, 2004.
[53] W. Dai and A. Wang, "Synthesis, characterization and properties of the DLC films with low Cr concentration doping by a hybrid linear ion beam system," Surface and Coatings Technology, vol. 205, pp. 2882-2886, 2011.
[54] Z. Y. Xu, Y. J. Zheng, H. Sun, L. Yong-xiang, and N. Huang, "Numerical and Experimental Study of Residual Stress of Multilayer Diamond-Like Carbon Films Prepared by Filtered Cathodic Vacuum Arc Deposition," Plasma Science, IEEE Transactions on, vol. 40, pp. 2261-2266, 2012.
[55] L. Zhang, H. Yang, X. Pang, K. Gao, and A. A. Volinsky, "Microstructure, residual stress, and fracture of sputtered TiN films," Surface and Coatings Technology, vol. 224, pp. 120-125, 2013.
[56] R. Anzalone, A. Alberti, and F. La Via, "Evaluation of 3C-SiC/Si residual stress and curvatures along different wafer direction," Materials Letters, vol. 118, pp. 130-133, 2014.
[57] R. Keys, "Cubic convolution interpolation for digital image processing," Acoustics, Speech and Signal Processing, IEEE Transactions on, vol. 29, pp. 1153-1160, 1981.
[58] J. Zhang, G. Jin, S. Ma, and L. Meng, "Application of an improved subpixel registration algorithm on digital speckle correlation measurement," Optics & Laser Technology, vol. 35, pp. 533-542, 2003.
[59] B. H. Friemel, L. N. Bohs, and G. E. Trahey, "Relative performance of two-dimensional speckle-tracking techniques: normalized correlation, non-normalized correlation and sum-absolute-difference," Ultrasonics Symposium, 1995. Proceedings., 1995 IEEE, vol. 2, pp. 1481-1484, 1995.
[60] D. Lecompte, A. Smits, S. Bossuyt, H. Sol, J. Vantomme, D. Van Hemelrijck, et al., "Quality assessment of speckle patterns for digital image correlation," Optics and Lasers in Engineering, vol. 44, pp. 1132-1145, 2006.
[61] S. Yaofeng and J. H. L. Pang, "Study of optimal subset size in digital image correlation of speckle pattern images," Optics and Lasers in Engineering, vol. 45, pp. 967-974, 2007.
[62] E. Kreyszig, Advanced engineering mathematics. New York, USA: John Wiley and Sons, Inc., 1999.
[63] C.-H. Chien and T.-H. Su, "Using DIC method for measuring residual stress in the nickel coating of the specimen," Experimental Techniques, 2015.
[64] R. C. Hibbeler, Mechanics of Materials: Prentice Hall, 2008.
[65] L. Gan, B. Ben-Nissan, and Ben-Davidb, "Modelling and finite element analysis of ultra-microhardness indentation of thin films," Thin Solid Films, vol. 290–291, pp. 362–366, 15 December 1996.
[66] J. Dolbow and M. Gosz, "Effect of out-of-plane properties of a polyimide film on the stress fields in microelectronic structures," Mechanics of Materials, vol. 23, pp. 311–321, August 1996.
[67] Plansee. http://www.plansee.com/cn/Materials-Chromium-939.htm.
[68] 李國誌, "應用數位影像關係法於微試件變形之量測," 機械工程學系, 成功大學, 2002.
[69] R. J. Moffat, "Contributions to the theory of single-sample uncertainty analysis," Journal of Fluids Engineering, vol. 104, pp. 250-258, 1982.
[70] 田春林, "光學薄膜應力與熱膨脹係數量測之研究," 光電科學系, 國立中央大學, 台灣,桃園, 2000.
[71] W. Water and S.-Y. Chu, "Physical and structural properties of ZnO sputtered films," Materials Letters, vol. 55, pp. 67–72, 2002.
[72] J. S. Milton and J. C. Arnold, Introduction to Probability and Statistics. 台灣,臺北市: McGrawHill, 2008.
[73] 賴儀聰, 樊丕緒, 熊樂群, 吳炎全, and 張達, "鎳鉻合金薄膜之退火熱處理製程等濺鍍參數研究," 機電科技研究所博, 國立台北科技大學 台灣,台北, 2006.
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